HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → (2,2-Diethoxyethyl)diethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Ethane, 2-bromo-1,1-diethoxy- | HCID 74852 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | (2,2-Diethoxyethyl)diethylamine | HCID 77164 | 20.8% |
Reaction Steps
2-bromo-1,1-diethoxyethane (10 g, 0.051 mol), diethylamine (11 g, 0.15 mol) and KI (8.5 g, 0.051 mol) were added in 100 mL acetone, and stirred for overnight at 40 degree. The resulting solution was filtered, concentrated and purified with silica gel column to give 2,2-diethoxy-N,N-diethylethanamine as brown oil 2.0 g (20.8% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388170B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-1d05ce371e2c4dfb971a0a1523dbdd3f |
| Source note | uspto-grants-2016_07 |