Dimethylamine → 4-Bromo-3-methoxy-N,N-dimethylbenzamide

HRID 1051852Notes

Reaction equation

HRID 1051852 reaction equation
[Br:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](O)=[O:7])=[CH:4][C:3]=1[O:11][CH3:12].[CH3:13][NH:14][CH3:15]>>[Br:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([N:14]([CH3:15])[CH3:13])=[O:7])=[CH:4][C:3]=1[O:11][CH3:12]

Participants

3

Reactant 2

HCID 674DimethylamineHCID 162158674-Bromo-3-methoxybenzoic acid

Product 1

HCID 467389714-Bromo-3-methoxy-N,N-dimethylbenzamide

Procedure

Starting with 4-bromo-3-methoxybenzoic acid and dimethyl amine, Int02.06 was prepared analogously to the procedure for the preparation of Int02.05.

Workup

  1. customwas prepared analogously to the procedure for the preparation of Int02.05

Sources & evidence

ORD record
ord-c9671ddebc554350b6dbf51bb9e304d7
Source dataset
uspto-grants-2016_07
Patent number
US09388177B2

Reaction notes

Loading…