HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl 4-formylpiperidine-1-carboxylate → HCID 118524559, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl 4-formylpiperidine-1-carboxylate | HCID 1514430 | — |
| Reactant | 4,5-Dibromobenzene-1,2-diamine | HCID 12196944 | — |
| Solvent | 2,2,2-Trifluoroethanol | HCID 6409 | — |
| Product | HCID 118524559 | HCID 118524559 | — |
Reaction Steps
4,5-dibromobenzene-1,2-diamine (100 mg, 0.38 mmol) and tert-butyl 4-formylpiperidine-1-carboxylate (160 mg, 0.76 mmol) were stirred for 1 hour in 2,2,2trifluoroethanol. Then Solvent was evaporated and product was purified on silica gel using EA/hex (1/1). Yield: 20 mg. m/z 657.1, rt. 4.2 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388192B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-260b732c123c41c4bb965af534b677e6 |
| Source note | uspto-grants-2016_07 |