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HRID1052377

反应详情

EQUATION

反应方程式

HRID 1052377 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(S(=O)(=O)Cl)cc1
HCID7401

4-Methoxybenzenesulphonyl chloride

C7H7ClO3S

结构：COc1ncc(B2OC(C)(C)C(C)(C)O2)cc1N
HCID59557920

2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-3-amine

C12H19BN2O3

PRODUCTS

生成物

1
结构：COc1ccc(S(=O)(=O)Nc2cc(B3OC(C)(C)C(C)(C)O3)cnc2OC)cc1
HCID89960828

未命名化合物

收率 80.3%

PROCEDURE

实验过程

2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-3-amine (200 mg, 0.8 mmol) was treated with 4-methoxybenzene-1-sulfonyl chloride (331 mg, 1.6 mmol) according to the method of Preparation 15b to give 270 mg (77% yield) of the title compound as an oil. Purity 96%.