HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluorobenzenesulfonyl Chloride → HCID 90102878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluorobenzenesulfonyl Chloride | HCID 2734273 | — |
| Reactant | 3-Amino-5-bromophenol | HCID 18388272 | — |
| Product | HCID 90102878 | HCID 90102878 | 121.5% |
Reaction Steps
3-Amino-5-bromophenol (600 mg, 2.87 mmol, prepared according to WO 2011119704 A1 20110929) was treated with 2,4-difluorobenzene-1-sulfonyl chloride (386 μl, 2.87 mmol) according to the method described in Preparation 15b to give 1.27 g (99% yield) of the title compound as an oil. Purity 70%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09388189B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-3890cf3f18404c9b9a33427ecb54e566 |
| Source note | uspto-grants-2016_07 |