HCID 86596495, compound → HCID 86596494, compound

Participants

Reaction Steps

A mixture of 9-anthrylmethyl N-[({tris[(2-{[(tris{[2-(methoxycarbonyl)ethoxy]methyl}methyl)amino]carbonyl}ethoxy)methyl]methyl}amino)carbonyl]propylcarbamate (0.60 g, 0.34 mmol) in acetone (30 ml) and 0.20 N NaOH (30 ml) was stirred at room temperature for 1 d, after which acetone was removed. The aqueous solution was washed with EA, stirred in an ice bath, acidified with dilute HCl, and extracted with EA. The organic layer was dried with MgSO4, filtered, and concentrated to yield 0.37 g (68% yield) of a yellow powder.

Provenance & Evidence