HCID 16681648, compound → HCID 64832775, compound

Participants

Reaction Steps

To a solution of product (4-B) (0.5 g 1.8 mmol) in MeOH (20 mL) was added Pd(OH)2/C (0.5 g) at rt. The reaction mixture was stirred at rt under H2 for about 1 h until complete consumption of product (4-B) by LC-MS. The reaction mixture was filtered, and the filtrate was concentrated to give crude product (5-B) (0.4 g, 90%) as a yellow solid. LC-MS (M-OH)+=232.

Provenance & Evidence