HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl phosphonoacetate → Methyl(E)-3-(2-methyl-5-nitro-phenyl)prop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl phosphonoacetate | HCID 80029 | — |
| Reactant | 2-Methyl-5-nitrobenzaldehyde | HCID 12654145 | — |
| Product | Methyl(E)-3-(2-methyl-5-nitro-phenyl)prop-2-enoate | HCID 118276893 | — |
Reaction Steps
Methyl(E)-3-(2-methyl-5-nitro-phenyl)prop-2-enoate (15a) is prepared from commercial 2-methyl-5-nitro-benzaldehyde (5j) (for a synthesis of (5j) see also Example 5, Method B) and commercial trimethyl phosphonoacetate as described in Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394236B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-e4bc85c6938d4d70842bbf91a719f581 |
| Source note | uspto-grants-2016_07 |