反应详情

To a suspension of 3-azido-6-(2-(benzyloxy)ethoxy)hexahydrofuro[3,2-b]furan (crude product) in MeOH (20 mL) was added Pd/C (10%, 0.31 g). The mixture was stirred at room temperature under a H2 atmosphere overnight. The mixture was filtered and washed with MeOH (20 mL). The filtrate was concentrated in vacuo to give the crude product as brown liquid. The residue was used in the next reaction without further purification.

1. filtrationThe mixture was filtered
2. washwashed with MeOH (20 mL)
3. concentrationThe filtrate was concentrated in vacuo