HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 44456226, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 5-((1H-imidazol-1-yl)methyl)-2-bromopyridine | HCID 70680985 | — |
| Product | HCID 44456226 | HCID 44456226 | — |
Reaction Steps
Synthesized using compound 1a (0.20 g, 0.84 mmol) and phenylboronic acid (0.20 g, 1.68 mmol) according to Method B. Yellow solid. Yield: 0.10 g, 57%. 1H NMR (CDCl3, 500 MHz): δH (ppm)=5.19 (s, 2H), 6.94 (t, J=1.3 Hz, 1H), 7.13 (s, 1H), 7.48-7.50 (m, 4H), 7.60 (s, 1H), 7.72 (d, J=8.2 Hz, 1H), 7.97-7.99 (m, 1H); 13C NMR (CDCl3, 125 MHz): δC (ppm)=48.1, 119.0, 120.6, 126.9, 128.8, 130.0, 130.4, 135.7, 137.3, 138.6, 148.6, 157.7; MS (ESI): m/z=236.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394290B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-02950e6bce0d446688933aa818ca5d61 |
| Source note | uspto-grants-2016_07 |