HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → 2-Bromo-3-(bromomethyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 2-Bromo-3-methylpyridine | HCID 220832 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 2-Bromo-3-(bromomethyl)pyridine | HCID 10901078 | — |
Reaction Steps
Synthesized from 2-bromo-3-methylpyridine (5.00 g, 29.1 mmol), NBS (5.69 g, 32.0 mmol) and DBPO (352 mg, 1.46 mmol) in CCl4 according to Method A. Yield: 2.87 g, 11.4 mmol, 39%. This compound was directly used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394290B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-6d31b88bbc234e6da3ea61156b70d883 |
| Source note | uspto-grants-2016_07 |