HRID1054939

反应详情

EQUATION

反应方程式

HRID 1054939 的结构方程式

PROCEDURE

实验过程

Was prepared in the same manner as described in General procedure 1d, using 3-Methyl-but-2-enoic acid 1-methylsulfanyl-1-pyrrolidin-1-yl-meth-(Z)-ylideneamide and methylhydrazine as starting materials. Extraction and evaporation of the solvents afforded 1-Methyl-5-(2-methyl-propenyl)-3-pyrrolidin-1-yl-1H-[1,2,4]triazole (261 mg/106%) as yellow oil. MS: m/z=207.1 (M+H+)

WORKUP

后处理

  1. customWas prepared in the same manner
  2. extractionExtraction and evaporation of the solvents