HRID1054939
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Was prepared in the same manner as described in General procedure 1d, using 3-Methyl-but-2-enoic acid 1-methylsulfanyl-1-pyrrolidin-1-yl-meth-(Z)-ylideneamide and methylhydrazine as starting materials. Extraction and evaporation of the solvents afforded 1-Methyl-5-(2-methyl-propenyl)-3-pyrrolidin-1-yl-1H-[1,2,4]triazole (261 mg/106%) as yellow oil. MS: m/z=207.1 (M+H+)
WORKUP
后处理
- customWas prepared in the same manner
- extractionExtraction and evaporation of the solvents