HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90032583, compound → HCID 72704899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90032583 | HCID 90032583 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 72704899 | HCID 72704899 | 55.2% |
Reaction Steps
(E)-5,6,8-Trimethyl-2-(2-(1-methyl-3-(pyrrolidin-1-yl)-1H-1,2,4-triazol-5-yl)vinyl)-[1,2,4]triazolo[1,5-a]pyrazine (45 mg, 99.4%) and Pd/C (5 mg) were stirred in acetic acid (0.7 ml) under hydrogen for 1 h. The mixture was filtered and concentrated to give the product (25 mg) as a light brown solid. MS: m/z=341.2 (M+H+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394311B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-c2ad09a2424f4e32a6cf3de2c67599cf |
| Source note | uspto-grants-2016_07 |