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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1054973Generated: November 1, 2026

HCID 90032583, compound → HCID 72704899, compound

https://huagongshe.com/reaction/1054973

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 90032583HCID 90032583—
CatalystPalladiumHCID 23938—
SolventAcetic AcidHCID 176—
ProductHCID 72704899HCID 7270489955.2%

Reaction Steps

(E)-5,6,8-Trimethyl-2-(2-(1-methyl-3-(pyrrolidin-1-yl)-1H-1,2,4-triazol-5-yl)vinyl)-[1,2,4]triazolo[1,5-a]pyrazine (45 mg, 99.4%) and Pd/C (5 mg) were stirred in acetic acid (0.7 ml) under hydrogen for 1 h. The mixture was filtered and concentrated to give the product (25 mg) as a light brown solid. MS: m/z=341.2 (M+H+)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09394311B2
Source datasetuspto-grants-2016_07
ORD IDord-c2ad09a2424f4e32a6cf3de2c67599cf
Source noteuspto-grants-2016_07