Sodium borohydride → HCID 90037884, compound

Participants

Reaction Steps

NaBH4 (7.81 mg, 0.206 mmol) was added to a solution of 2-chloro-1-(phenylsulfonyl)-1H-indole-3-carbaldehyde (33 mg, 0.103 mmol) in DCM/MeOH 1:1 (10 mL). After 16 h the mixture was diluted with sat. NH4Cl and EtOAc, the organic layer separated and washed with H2O, dried over MgSO4, filtered and the filtrate concentrated to give the title compound (33 mg, 99%) which was used without purification.

Provenance & Evidence