HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyano-5-(trifluoromethyl)benzoic acid → HCID 89700019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyano-5-(trifluoromethyl)benzoic acid | HCID 58902287 | — |
| Reactant | 4-Methyl-3-[6-(pyridin-3-yl)-1H-imidazo[1,2-b]pyrazol-1-yl]aniline | HCID 89700023 | — |
| Product | HCID 89700019 | HCID 89700019 | — |
Reaction Steps
Analogously to the process described in Example 26, 80 mg (0.276 mmol) of the compound of Example 6A and 60 mg (0.276 mmol) of the compound of Example 42A gave 72 mg (54% of theory) of the title compound. In this case, the reaction time was 18 h, and subsequent trituration of the product with diisopropyl ether could be dispensed with.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394309B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-425695ee911c474597cbcc5613ecc7de |
| Source note | uspto-grants-2016_07 |