HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Isothiocyanato-2-(2-methoxyethoxyl)ethane → 8-iodo-3-(2-(2-methoxyethoxyl)ethyl)-2-(methyl-thio)quinazolin-4(3H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Isothiocyanato-2-(2-methoxyethoxyl)ethane | HCID 22101683 | — |
| Reactant | 8-iodo-3-(2-methoxyethyl)-2-(methylthio)quinazolin-4(3H)-one | HCID 89781985 | — |
| Product | 8-iodo-3-(2-(2-methoxyethoxyl)ethyl)-2-(methyl-thio)quinazolin-4(3H)-one | HCID 89782139 | — |
Reaction Steps
This compound (0.81 g, 1.92 mmol) was prepared according to the procedures described for Intermediate 715a, starting from 1-isothiocyanato-2-(2-methoxyethoxyl)ethane (716a; 0.67 g, 4.21 mmol). m/z (ESI, +ve ion) 421.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09394297B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-11c5ccb481894f92b4984c0ad2ae4638 |
| Source note | uspto-grants-2016_07 |