HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86663089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-Chloro-3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carboxylic acid | HCID 19754693 | — |
| Product | HCID 86663089 | HCID 86663089 | — |
Reaction Steps
3.2 g of 5-chloro-3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carboxylic acid and 44.3 ml of thionyl chloride were refluxed for 5 hours. After cooling down, the reaction mixture was evaporated under vacuum to yield 3.5 g of 5-chloro-3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carbonyl chloride as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09398767B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-60cfd843226345f9939822a6d3dadd0e |
| Source note | uspto-grants-2016_07 |