Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| Reactant | HCID 66686510 | HCID 66686510 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86663090 | HCID 86663090 | — |
Reaction Steps
A solution of 140 mg (0.31 mmol) of phosphorus pentasulfide and 500 mg (1.26 mmol) of N-cyclopropyl-3-(difluoromethyl)-5-fluoro-1-methyl-N-[2-(trimethylsilyl)benzyl]-1H-pyrazole-4-carboxamide in 20 ml of dioxane was heated at 100° C. for 2.5 hours. 2 ml of water were then added and the reaction mixture was heated at 100° C. for another 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09398767B2 |
|---|
| Source dataset | uspto-grants-2016_07 |
|---|
| ORD ID | ord-c92d28161c444439a5decbd32300906e |
|---|
| Source note | uspto-grants-2016_07 |
|---|
