HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxypropylamine → HCID 118566613, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxypropylamine | HCID 1672 | — |
| Reactant | 2,6-Dichloro-quinoline-5-carboxylic acid (4,4-difluorocyclohexylmethyl)-amide | HCID 118555965 | — |
| Product | HCID 118566613 | HCID 118566613 | — |
Reaction Steps
The title compound was synthesized according to the procedure described in example 1 using 2,6-dichloro-quinoline-5-carboxylic acid (4,4-difluoro-cyclohexylmethyl)-amide, and 3-methoxy-propylamine. 1H NMR (400 MHz, DMSO-d6) δ ppm 8.70 (t, J=5.8 Hz, 1H), 7.59 (d, J=9.2 Hz, 1H), 7.47-7.50 (m, 2H), 7.24 (t, J=5.4 Hz, 1H), 6.82 (d, J=9.2 Hz, 1H), 3.39-3.42 (m, 4H), 3.20-3.22 (m, 5H), 2.01-2.03 (m, 2H), 1.73-1.85 (m, 7H), 1.22-1.31 (m, 2H). m/z: 426.0 [M+H]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09399623B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-9bdf5831673c4ef495d5a0b1dd6410fa |
| Source note | uspto-grants-2016_07 |