HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 77230946, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 77230948 | HCID 77230948 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 77230946 | HCID 77230946 | — |
Reaction Steps
To a solution of 4-oxo-6-phenyl-4H-pyran-3-yl acetate (100 mg, 0.4 mmol) in MeOH (10.9 mL) is added K2CO3 (180 mg, 1.3 mmol) and the reaction was stirred for 15 min at room temperature. The reaction mixture was concentrated under reduced pressure to provide 5-hydroxy-2-phenyl-4H-pyran-4-one which was used in the subsequent step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09399651B2 |
| Source dataset | uspto-grants-2016_07 |
| ORD ID | ord-54289ab56780471fb9d73d45025e84d6 |
| Source note | uspto-grants-2016_07 |