Ethanethiol → 4-Bromo-3-(ethylthio)-N-methyl-2-nitroaniline

HRID 1057012Notes

Reaction equation

HRID 1057012 reaction equation
[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1F.[CH2:14]([SH:16])[CH3:15]>>[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1[S:16][CH2:14][CH3:15]

Participants

3

Reactant 2

HCID 6343EthanethiolHCID 1180938324-Bromo-3-fluoro-N-methyl-2-nitroaniline

Product 1

HCID 1180938874-Bromo-3-(ethylthio)-N-methyl-2-nitroaniline

Procedure

This compound was synthesized according to the procedure of Example 11, Step 1, using 4-bromo-3-fluoro-N-methyl-2-nitroaniline and ethanethiol as the starting materials. LCMS calculated for C9H12BrN2O2S (M+H)+: m/z=291.0, 293.0. found: 290.9, 292.9.

Workup

  1. customThis compound was synthesized

Sources & evidence

ORD record
ord-bb6929217e8640c397b1b8c55ef1db52
Source dataset
uspto-grants-2016_07
Patent number
US09399640B2

Reaction notes

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