Methyl iodide → HCID 118093842, compound

HRID 1057014Notes

Reaction equation

HRID 1057014 reaction equation
[Br:1][C:2]1[CH:3]=[CH:4][C:5]2[O:10][CH2:9][C:8](=[O:11])[NH:7][C:6]=2[C:12]=1[O:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.[CH3:20]I>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]2[O:10][CH2:9][C:8](=[O:11])[N:7]([CH3:20])[C:6]=2[C:12]=1[O:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 118093821HCID 118093821, compound

Product 1

HCID 118093842HCID 118093842, compound

Procedure

This compound was synthesized according to the procedure of Example 83, Step 1, using 6-bromo-5-phenoxy-2H-1,4-benzoxazin-3(4H)-one and methyl iodide as the starting materials. LCMS calculated for C18H13BrNO3 (M+H)+: m/z=334.0, 336.0. found: 333.9, 335.9.

Workup

  1. customThis compound was synthesized

Sources & evidence

ORD record
ord-c95e8e0208fe48c79319326d01042c3b
Source dataset
uspto-grants-2016_07
Patent number
US09399640B2

Reaction notes

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