HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,5,5,8,8-Pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)boronic acid → HCID 22634659, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,5,5,8,8-Pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)boronic acid | HCID 10037535 | — |
| Reactant | HCID 22634694 | HCID 22634694 | — |
| Product | HCID 22634659 | HCID 22634659 | — |
Reaction Steps
In a similar manner to Example 9(b), by reaction of 73.4 g (0.30 mol) of 3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthylboronic acid with 44.7 g (0.20 mol) of 4-bromophenylacrylic acid, and after recrystallization from ethanol, 48 g (61%) of 3-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-naphthyl)phenylacrylic acid are obtained, with a melting point of 207-8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06515021B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-a9778c6040984203842439444e574312 |
| Source note | uspto-grants-2003_02 |