HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-[1-oxo-3-(3-hydroxyphenyl)propyl]benzoic acid → 2-Chloro-4-(1-hydroxy-3-(3-hydroxyphenyl)propyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-[1-oxo-3-(3-hydroxyphenyl)propyl]benzoic acid | HCID 22661377 | — |
| Reactant | 2-Chloro-4-[1-hydroxy-3-(3-hydroxyphenyl)propyl]benzoic acid, methyl ester | HCID 23560778 | — |
| Product | 2-Chloro-4-(1-hydroxy-3-(3-hydroxyphenyl)propyl)benzoic acid | HCID 22661228 | 90% |
Reaction Steps
This compound was prepared in 90% yield from rac.-2-chloro-4-[1-hydroxy-3-(3-hydroxyphenyl)propan-1-yl]benzoic acid, methyl ester (Example 94) by the procedure described for 2-chloro-4-[3-(3-hydroxyphenyl)-1-oxopropan-1-yl]benzoic acid (Example 95). The product was a racemic mixture and was not resolved.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06515124B2 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-6acf587498cb410dbcedcef0982dc579 |
| Source note | uspto-grants-2003_02 |