Dipropylamine → HCID 18669011, compound

Participants

Reaction Conditions

Reaction Steps

2-Fluoro-5-nitrobenzaldehyde (48 mg, 0.28 mmol) was dissolved in N,N-dimethylformamide (2.4 mL), and di-n-propylamine (0.15 mL, 1.1 mmol) and potassium carbonate (0.16 g, 1.1 mmol) were added thereto, followed by stirring at 25° C. for 1 hour. After the conventional post-reaction treatment, the residue was purified by silica gel chromatography(eluted with chloroform), to obtain 2-(N,N-di-n-propylamino)-5-nitrobenzaldehyde (49 mg, 69%).

Provenance & Evidence