Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1058996Generated: November 2, 2026

Dichloromethane → HCID 9839612, compound

https://huagongshe.com/reaction/1058996

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 9907496HCID 9907496—
ProductHCID 9839612HCID 983961275%

Reaction Steps

A solution of (±)-(1S,2S,3R,4R)-3-Acetamidomethyl-2-(N-t-butoxycarbonylamino)methyl-4-methoxycarbonylcyclopentane-1-carboxylic acid (62 mg, 0.16 mmol) in of dichloromethane (4 mL) was reacted with trifluoroacetic acid (1.0 mL) for 1 hour, at room temperature. The solution was concentrated in vacuo, at 25° C. The residue was treated with 1 N HCl and concentrated in vacuo to provide the title compound as a white solid (yield: 39 mg, 75%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06518305B1
Source datasetuspto-grants-2003_02
ORD IDord-d270fb4601da479ba6bf2cf89316ef32
Source noteuspto-grants-2003_02