HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 22322416, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 1-Boc-4-[(3,4-dichlorophenyl)amino]-piperidine | HCID 22322413 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22322416 | HCID 22322416 | — |
Reaction Steps
The product of step (i) above (6.5 g) was dissolved in dichloromethane (75 ml) and trifluoroacetic acid (25 ml) added. After 72 hours at room temperature the solution was evaporated and the residue triturated under ether to give the sub-titled product as a solid (6.3 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518286B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-159510e01b994c90b11835429beb2c43 |
| Source note | uspto-grants-2003_02 |