HCID 9839601, compound → HCID 9839600, compound

HRID 1059034Notes

Reaction equation

HRID 1059034 reaction equation
[OH:1][CH:2]([C:14]1[CH:19]=[CH:18][C:17]([OH:20])=[C:16]([O:21][CH3:22])[CH:15]=1)[C:3](=[O:13])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].CN(C(C#N)CCCCCCCCC)C>>[OH:13][CH:3]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[C:2]([C:14]1[CH:19]=[CH:18][C:17]([OH:20])=[C:16]([O:21][CH3:22])[CH:15]=1)=[O:1]

Participants

3

Reactant 2

HCID 9839601HCID 9839601, compoundHCID 11708298HCID 11708298, compound

Product 1

HCID 9839600HCID 9839600, compound

Procedure

Similar procedure was used to synthesise 1-hydroxy-1-(4-hydroxy-3-methoxyphenyl)undecan-2-one where 1-(N,N-dimethylamino)-1-decylcyanide was formed instead and reacted with vanillin-THP.

Workup

  1. customwas formed instead

Sources & evidence

ORD record
ord-7f13b27cac954ee8aafbb1e9552ea9bb
Source dataset
uspto-grants-2003_02
Patent number
US06518315B1

Reaction notes

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