3-Chloro-2-methyl-1-propene → N-methallyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine

HRID 1059037Notes

Reaction equation

HRID 1059037 reaction equation
[CH2:1]([O:4][N:5]([C:16]([CH3:19])([CH3:18])[CH3:17])[C:6]([CH3:15])([CH3:14])[C:7]([NH:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:8])[CH:2]=[CH2:3].[C:20](N(C(C)(C)C(NC(C)(C)C)=O)O)(C)(C)C.C(Cl)C(=C)C>>[CH2:1]([O:4][N:5]([C:16]([CH3:19])([CH3:18])[CH3:17])[C:6]([CH3:15])([CH3:14])[C:7]([NH:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:8])[C:2](=[CH2:20])[CH3:3]

Participants

4

Reactant 3

HCID 112413-Chloro-2-methyl-1-propeneHCID 11207972N-allyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amineHCID 22182216Tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine

Product 1

HCID 23563825N-methallyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amineYield 84%

Procedure

The compound is prepared in analogy to compound (204) from tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine and methallylchloride in 84% yield as colorless oil.

Sources & evidence

ORD record
ord-379597fab6b9495dad5b9a0e2fffc288
Source dataset
uspto-grants-2003_02
Patent number
US06518326B1

Reaction notes

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