HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorooxane → N-(2-tetrahydropyranyloxy)-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorooxane | HCID 524400 | — |
| Reactant | N-allyloxy-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine | HCID 11207972 | — |
| Reactant | Tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine | HCID 22182216 | — |
| Product | N-(2-tetrahydropyranyloxy)-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine | HCID 22598546 | 33% |
Reaction Steps
The compound is prepared in analogy to compound (204) from tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine and 2-chlor-tetrahydropyrane in 33% yield as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518326B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-5f1bdc211ec540fda274bab5a12d973a |
| Source note | uspto-grants-2003_02 |