HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Acetamidophenyl)boronic acid → HCID 18668639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Acetamidophenyl)boronic acid | HCID 157274 | — |
| Reactant | 1-(4-bromophenyl)-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanol | HCID 12043387 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Product | HCID 18668639 | HCID 18668639 | 96.1% |
Reaction Steps
By the reaction in the same manner as in Example 4-(ii) using 1-(4-bromophenyl)-2-methyl-1-(1-trityl-1H-imidazol-4-yl)-1-propanol (1.04 g), 3-(acetylamino)phenylboronic acid (571 mg) and tetrakis(triphenylphosphine)palladium(0) (301 mg), the title compound (1.10 g) was obtained as a pale-yellow amorphous powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518257B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-78c06acec4434a378a6617410343488d |
| Source note | uspto-grants-2003_02 |