HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → N-(3-bromo-4-methoxyphenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-Bromo-4-nitroanisole | HCID 78870 | — |
| Catalyst | Iron | HCID 23925 | — |
| Product | N-(3-bromo-4-methoxyphenyl)acetamide | HCID 244158 | — |
Reaction Steps
By the reaction in the same manner as in Example 33-(i) using 2-bromo-4-nitroanisole (5.41 g), iron powder (6.49 g) and acetic anhydride (4.4 ml), the title compound (4.87 g) was obtained as a colorless powder crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518257B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-86b40695a4af4a518e8fd0c57262b5ed |
| Source note | uspto-grants-2003_02 |