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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1059216Generated: October 27, 2026

2-(3-bromophenyl)-N-methylacetamide → HCID 18668613, compound

https://huagongshe.com/reaction/1059216

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(3-bromophenyl)-N-methylacetamideHCID 18668529—
Reactant4-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl]phenylboronic acidHCID 18668578—
CatalystHCID 178418397HCID 178418397—
ProductHCID 18668613HCID 1866861323.5%

Reaction Steps

By the reaction in the same manner as in Example 33-(ii) using 4-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl]phenylboronic acid (3.47 g), 2-(3-bromophenyl)-N-methylacetamide (0.93 g) and tetrakis(triphenylphosphine)palladium(0) (0.21 g), the title compound (580 mg) was obtained as colorless powder crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06518257B1
Source datasetuspto-grants-2003_02
ORD IDord-9700cb29194447428dbd7dc8793de71f
Source noteuspto-grants-2003_02