HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 178466227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 1-{4'-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl][1,1'-biphenyl]-3-yl}ethanone | HCID 18668620 | — |
| Product | HCID 178466227 | HCID 178466227 | 47.6% |
Reaction Steps
By the reaction in the same manner as in Example 4-(iii) using 1-{4′-[1-hydroxy-2-methyl-1-(1-trityl-1H-imidazol-4-yl)propyl][1,1′-biphenyl]-3-yl}ethanone (3.30 g) and pyridine hydrochloride (870 mg), the title compound (910 mg) was obtained as a colorless amorphous powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06518257B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-40b389ce1d44417f81e673b56147f226 |
| Source note | uspto-grants-2003_02 |