Methanol → HCID 23565315, compound

Participants

Reaction Steps

To a solution of 0.486 g of (1-benzyl-4-vinylpiperidin-4-yl)acetaldehyde in N,N-dimethylformamide (10 ml) were added 0.48 g of methanol and 4.50 g of pyridinium dichromate and the resulting mixture was stirred at room temperature for 20 hours. After adding 100 ml of diethyl ether, the reaction mixture was filtered through celite. After concentrating under reduced pressure, the residue was purified by silica gel column chromatography (eluted with dichloromethane/methanol) to thereby give 0.321 g of the title compound as a colorless oily substance.

Provenance & Evidence