2-Nitroaniline → HCID 18670474, compound

HRID 1059377Notes

Reaction equation

[N+:1]([C:4]1[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=1[NH2:6])([O-:3])=[O:2].[Cl:11][C:12]1[C:17](Cl)=[N:16][CH:15]=[CH:14][N:13]=1>>[N+:1]([C:4]1[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=1[NH:6][C:17]1[C:12]([Cl:11])=[N:13][CH:14]=[CH:15][N:16]=1)([O-:3])=[O:2]

Participants

Reactant 2

HCID 69462-Nitroaniline

HCID 785752,3-Dichloropyrazine

Product 1

HCID 18670474HCID 18670474, compoundYield 67.6%

Procedure

Starting with 41.4 g of 2-nitroaniline and 35.0 g of 2,3-dichloropyrazine, 39.8 g of the title compound was obtained by the same method as the one described in Production Example 120.

Sources & evidence

ORD record: ord-1908fcc3b7c64b6aa11cc23cc5c814cf
Source dataset: uspto-grants-2003_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06518423B1

Reaction notes

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