Dimethylamine → HCID 18670396, compound

HRID 1059379Notes

Reaction equation

HRID 1059379 reaction equation
Br[CH2:2]/[CH:3]=[CH:4]/[CH2:5][N:6]([C:16]1[C:21]([Cl:22])=[N:20][CH:19]=[CH:18][N:17]=1)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[N+:13]([O-:15])=[O:14].[CH3:23][NH:24][CH3:25]>C(O)C>[CH3:23][N:24]([CH3:25])[CH2:2]/[CH:3]=[CH:4]/[CH2:5][N:6]([C:16]1[C:21]([Cl:22])=[N:20][CH:19]=[CH:18][N:17]=1)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[N+:13]([O-:15])=[O:14]

Participants

4

Reactant 2

HCID 674DimethylamineHCID 18670107HCID 18670107, compound

Product 1

HCID 18670396HCID 18670396, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

Similar to Example 1094, 0.34 g of (E)-2-[N-(4-bromo-2-buten-1-yl)-N-(2-nitrophenyl)amino]-3-chloropyrazine was treated with 20 ml of a 0.86 M ethanol solution of dimethylamine in 5 ml of ethanol to thereby give 0.17 g of the title compound as a yellow oily substance.

Sources & evidence

ORD record
ord-827a8a9955e04e2c9e4994795b13d800
Source dataset
uspto-grants-2003_02
Patent number
US06518423B1

Reaction notes

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