Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 12056724 | HCID 12056724 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15452301 | HCID 15452301 | — |
Reaction Steps
In 20 ml of toluene were dissolved 2-phenylethylamine (0.6 g) and triethylamine (0.6 g), then, 4-chloro-6-(1-acetoxy-ethyl)-5-iodopyrimidine (1.7 g) was added to the solution, and the mixture was heated at about 60° C. for 3 hours while stirring.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06521627B1 |
|---|
| Source dataset | uspto-grants-2003_02 |
|---|
| ORD ID | ord-07824c3545e941d09a80a23c0e44c201 |
|---|
| Source note | uspto-grants-2003_02 |
|---|
