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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1059690Generated: October 31, 2026

Phenethylamine → HCID 12056726, compound

https://huagongshe.com/reaction/1059690

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenethylamineHCID 1001—
ReactantTriethylamineHCID 8471—
ReactantHCID 12056725HCID 12056725—
SolventTolueneHCID 1140—
ProductHCID 12056726HCID 12056726—

Reaction Conditions

Temperature60 °C

Reaction Steps

In 20 ml of toluene were dissolved 2-phenylethylamine (0.6 g) and triethylamine (0.6 g), then, 4-chloro-6-(1-hydroxy-ethyl)-5-iodopyrimidine (1.4 g) was added to the solution, and the mixture was heated at about 60° C. for 3 hours while stirring.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06521627B1
Source datasetuspto-grants-2003_02
ORD IDord-105fa118dd3b493d8fb7c0379f146c71
Source noteuspto-grants-2003_02