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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1059727Generated: November 3, 2026

Sodium Bicarbonate → HCID 22168674, compound

https://huagongshe.com/reaction/1059727

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 22168559HCID 22168559—
SolventMethanolHCID 887—
ProductHCID 22168674HCID 22168674—

Reaction Steps

Reduction of the above nitro compound by the method of Example 2, except that the solvent was methanol, and NaHCO3 solution was used to basify, gave allyl 2-allyloxy-5-aminobenzoate. Nmr (CDCl3): δ 3.23 (br, 2H); 4.53 (dt, 2H); 4.79 (d, 2H); 5.21-5.49 (m, 4H); 5.93-6.14 (m, 2H); 6.80 (m, 2H); 7.16 (d, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06521612B2
Source datasetuspto-grants-2003_02
ORD IDord-b535b67e408c4358991cd58bd040cd18
Source noteuspto-grants-2003_02