HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl (bis(2-methoxyethyl)amino)acetate → (Bis(2-methoxyethyl)amino)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl (bis(2-methoxyethyl)amino)acetate | HCID 53622886 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (Bis(2-methoxyethyl)amino)acetic acid | HCID 9815497 | — |
Reaction Steps
A solution of Example 81A (19.4 g; 69 mmol) and 10% Pd/C (3.5 g) in methanol (150 mL) at room temperature was stirred under 4 atm of H2 for 17 hours, filtered through diatomaceous earth (Celite®), and concentrated to provide the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521658B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-b8c16ed14b5c49159d2334e7dc94ba7a |
| Source note | uspto-grants-2003_02 |