HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Methoxypyridin-2-yl)-nitrobenzene → 3-(4-Methoxypyridin-2-yl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Methoxypyridin-2-yl)-nitrobenzene | HCID 18667584 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(4-Methoxypyridin-2-yl)aniline | HCID 18667489 | 100.3% |
Reaction Steps
A suspension of 3-(4-methoxypyridin-2-yl)nitrobenzene (1.8 g) in ethanol (40 ml) was hydrogenated over palladium on carbon (10% w/w, 50% wet, 800 mg) under a hydrogen atmosphere for 5 hours. The catalyst was filtered off, and the filtrate was evaporated under reduced pressure to give 3-(4-methoxypyridin-2-yl)aniline (1.57 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521643B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-61a70675b81949c597523928ecb22736 |
| Source note | uspto-grants-2003_02 |