HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Ethoxypyridin-2-yl)nitrobenzene → 3-(4-Ethoxypyridin-2-yl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Ethoxypyridin-2-yl)nitrobenzene | HCID 18667579 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(4-Ethoxypyridin-2-yl)aniline | HCID 18667629 | 100.3% |
Reaction Steps
A suspension of 3-(4-ethoxypyridin-2-yl)nitrobenzene (0.3 g) in ethanol (6 ml) was hydrogenated over palladium on carbon (10% w/w, 50% wet, 0.2 g) under a hydrogen atmosphere for 3 hours. The catalyst was filtered off, and the filtrate was evaporated under reduced pressure to give 3-(4-ethoxypyridin-2-yl)aniline (0.264 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521643B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-3835b13a896b4ea49d3c9b17e10c2f25 |
| Source note | uspto-grants-2003_02 |