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HRID10600

反应详情

EQUATION

反应方程式

HRID 10600 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NCc1ccc(CN)cc1
HCID3354775

1-(N-Boc-aminomethyl)-4-(aminomethyl)benzene

C13H20N2O2

结构：Cl.O=S(=O)(Cl)c1cccc2cnccc12
HCID13116932

Isoquinoline-5-sulfonyl chloride--hydrogen chloride (1/1)

C9H7Cl2NO2S

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCc1ccc(CNS(=O)(=O)c2cccc3cnccc23)cc1
HCID69523966

未命名化合物

收率 82.7%

PROCEDURE

实验过程

According to Reference Example 5, Step B, a reaction was performed by using isoquinoline-5-sulfonyl chloride hydrochloride (10 g) and Intermediate 59 (8.96 g) to obtain the title compound (13.39 g).