HuagongsheHuagongshe Chemistry Print Report · For research reference only
E-7-Phenylhept-4-enoic acid → 7-Phenyl heptanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | E-7-Phenylhept-4-enoic acid | HCID 9899164 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 7-Phenyl heptanoic acid | HCID 520987 | — |
Reaction Steps
7-Phenylheptanoic acid was prepared from E-7-phenylhept-4-enoic acid by hydrogenation at 40 psi using 5% palladium on carbon as the catalyst. Quantitative conversion of the alkene to the alkane was observed by thin layer chromatographic analysis. The product acid was purified by chromatography on silica gel and fully characterized by spectroscopic methods (infrared and nuclear magnetic resonance) and combustion analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521664B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-d56d32c21b934fbe8c7bec70ebcbd1b8 |
| Source note | uspto-grants-2003_02 |