HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 18630246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 2-(Trifluoromethyl)benzoyl chloride | HCID 67561 | — |
| Product | HCID 18630246 | HCID 18630246 | 67% |
Reaction Steps
2-(Trifluoromethyl)benzoyl chloride and ethyl amine were combined according to General Method E1 and recrystallized from cold hexanes to give 7.7 g N-ethyl-2-(trifluoromethyl)benzamide as a white solid, a 67% yield. m.p. 73-76° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521603B2 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-cea46084002c4f78a6735832ed55dfb7 |
| Source note | uspto-grants-2003_02 |