HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 22283164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 22283057 | HCID 22283057 | — |
| Product | HCID 22283164 | HCID 22283164 | — |
Reaction Steps
Using 4-Methoxy-7-phenoxy-benzothiazol-2-ylamine and benzoyl chloride the title compound was obtained crude, which was chromatographed over SiO2 (Merck 230-400 mesh) eluting with CH2Cl2/EtOAc (1:1), to afford the pure title compound as a white solid (72% yield), MS: m/e=376.1 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521754B2 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-4c6fa90859b84a53ad6329167d875d21 |
| Source note | uspto-grants-2003_02 |