Carbamate → HCID 22283357, compound
Reaction equation
[C:1](=[O:4])([O-])N.[CH3:5][O:6][C:7]1[C:12]2[N:13]=[C:14]([NH:16][C:17](=[O:19])[OH:18])[S:15][C:11]=2[CH:10]=[CH:9][CH:8]=1>>[CH3:5][O:6][C:7]1[C:12]2[N:13]=[C:14]([NH:16][C:17](=[O:18])[OH:19])[S:15][C:11]=2[C:10]([N:13]2[CH2:14][CH2:1][O:4][CH2:11][CH2:12]2)=[CH:9][CH:8]=1Participants
3
Procedure
Carbamate formation using the same procedure as for (4-methoxy-benzothiazol-2-yl)-carbamic acid methyll ester yields the product as off-white solid in 58% yield. MS: m/e=324 (M+H+).
Sources & evidence
- ORD record
- ord-ece2b9322e8e4e9c9b72a23076662a2e
- Source dataset
- uspto-grants-2003_02
- Patent number
- US06521754B2
Reaction notes
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