HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → N-(2,6-Dichlorobenzoyl)-4-(2-hydroxymethyl-3-thienyl)-L-phenylalanine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | N-(2,6-Dichlorobenzoyl)-4-(2-formyl-3-thienyl)-L-phenylalanine methyl ester | HCID 54164979 | — |
| Product | N-(2,6-Dichlorobenzoyl)-4-(2-hydroxymethyl-3-thienyl)-L-phenylalanine | HCID 53842613 | — |
Reaction Steps
The title compound was prepared by NaBH4 reduction of N-(2,6-Dichlorobenzoyl)-4-(2-formyl-3-thienyl)-L-phenylalanine methyl ester followed by hydrolysis as described in Example 50. ESMS m/z 472 (M++Na), 448 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06521666B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-05ca3aca70574d12946d2caf6e322a67 |
| Source note | uspto-grants-2003_02 |