HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzaldehyde → 2-(4-Nitrobenzylidene)amino-3,3-dichloropropenonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | 2-Amino-3,3-dichloroprop-2-enenitrile | HCID 12257120 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-(4-Nitrobenzylidene)amino-3,3-dichloropropenonitrile | HCID 12290720 | — |
Reaction Steps
A solution of 2-amino-3,3-dichloropropenonitrile (15.0 g, 0.11 mole) and 4-nitrobenzaldehyde (15.1 g, 0.10 mmol) in toluene (200 ml) was refluxed for 23 hours. The mixture was evaporated, methanol (100 ml) was added and the mixture was allowed to stand overnight. After filtration, the title compound was isolated as a brown-yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06524552B2 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-d27838256c1e4ffd9ab86d04f0ff20c9 |
| Source note | uspto-grants-2003_02 |